{
"$type": "site.standard.document",
"description": "An effectively solvent-free alkali metal or alkali earth metal closo-borate salt is prepared in the presence of a non-aqueous solvent where the solvent can be removed to levels below one mole percent of the salt. The process involves the exchange of cations with a closo-borate anion via an…",
"path": "/patents/1308964",
"publishedAt": "2022-01-20T00:00:00.000Z",
"site": "at://did:plc:oql6ds5vnff4ugar6rruliwd/site.standard.publication/3mn3ohu7oxx5w",
"tags": [
"C01D15/00",
"Toyota Motor Engineering & Manufacturing North America, Inc."
],
"textContent": "An effectively solvent-free alkali metal or alkali earth metal closo-borate salt is prepared in the presence of a non-aqueous solvent where the solvent can be removed to levels below one mole percent of the salt. The process involves the exchange of cations with a closo-borate anion via an acid-base process or a metathesis process. The solvent is removed from the alkali metal or alkali earth metal closo-borate salt by heating. The temperature can be greater than the melting point of the salt but lower than temperatures where decomposition occurs.",
"title": "METHOD FOR SYNTHESIS OF SOLVENT-FREE LITHIUM BORON CLUSTER BASED SALTS"
}