METHOD FOR PRODUCING ELECTRODE CATALYST, METHOD FOR PRODUCING GAS DIFFUSION ELECTRODE, AND METHOD FOR PRODUCING FILM-ELECTRODE JOINT BODY

DRIVE January 29, 2025
Source
An object of the present invention is to provide a method of producing an electrode catalyst having excellent catalytic activity and excellent durability in an electrode catalyst layer of MEA for a PEFC. The present invention provides a method of producing an electrode catalyst having a porous carbon support that has nanopores having a pore diameter of 1 to 20 nm, micropores having a pore diameter of less than 1 nm, and a BET specific surface area (nitrogen adsorption specific surface area) of 1000 to 1500 m2/g, and catalyst particles containing Pt supported on the support, including: a first step for preparing a powder in which the catalyst particles are supported on the support by using the support and raw materials of the catalyst particle; and a second step for accommodating the powder obtained through the first step in a flow-type reactor, flowing ammonia gas through the reactor under conditions of a concentration of 10 to 100% and a pressure of 0.1 MPa to 0.5 MPa, and regulating the temperature in the reactor to 500 °C or more and less than the decomposition temperature of ammonia, keeping for 5 to 10 hours to chemically react the powder and the ammonia gas.

Discussion in the ATmosphere

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